Name of the Experiment:
Identification of given textile fiber sample.
Introduction:
The identification of textile fibers is a task frequently performed in a textile lab. The need to identify fibers arises in fibers research as well as during fabric production and processing. The identification of an unknown fiber in a yarn or fabric made up of a mixture of fibers is also often carried out. Identification tests are performed by utilizing tests that take advantage of the different chemical (and to some extent physical) characteristics of textile fibers.
The properties of the yarn and fabric are directly influenced by the properties of fiber from which yarn and fabric are made. There are different methods of fibre identification for characterization of the structural, physical, and chemical properties of fibers. Several methods are used to identify fibers and to differentiate them from one another. The most common methods include microscopic examination, solubility tests, heating and burning characteristics, density or specific gravity, and staining techniques. In this experiment I will discuss identification of thermoplastic and non thermoplastic textile fiber.
Objectives:
- To know about the physical properties of textile fiber sample.
- To know about the chemical properties of textile fiber sample.
- To identify the type of sample fiber.
Sample_01
Visual properties:
- Color: White
- Handle: Harsh
Physical test:
Preliminary sorting test by heating:
We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:
Obs. no. | Behavior | Remark |
1 | Does not shrink from flame or melt | Non-thermoplastic |
For non- thermoplastic fiber:
Bring a small tuft of fibers into a small non-luminous flame –
Obs. no. | Behavior | Remark |
1 | Burn with irregular spurting flame, leaving a black inflated, easily powdered residue & emits a smell of burnt hair. | Protein (Silk & Wool) |
Chemical test:
Obs. no. | Chemical | Behavior | Remark | |
Cold | Hot | |||
1. | Phenol | Unchanged | Unchanged | |
2. | Dimethyl formamide | Unchanged | Unchanged | |
3. | Sulphuric acid | Unchanged | Dissolve | May be silk |
4. | Sodium hydroxide | Unchanged | Dissolve | May be wool |
Confirmation test:
Obs. no. | Chemical | Behavior | Result | |
Cold | Hot | |||
1. | Sodium hydroxide | Unchanged | Dissolve | Wool |
Sample_02
Visual properties:
- Color: White
- Handle: Soft handle
Physical test:
Preliminary sorting test by heating:
We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:
Obs. no. | Behavior | Remark |
1. | Does not shrink from flame or melt | Non-thermoplastic |
For non- thermoplastic fiber:
Bring a small tuft of fibers into a small non-luminous flame –
Obs. no. | Behavior | Remark |
1. | Burns readily and without melting, emitting a smell of burnt paper & leaving a small amount of ash. | Cellulose & Regenerated Cellulose |
Chemical test:
Obs. no. | Chemical | Behavior | Remark | |
Cold | Hot | |||
1. | Phenol | Unchanged | Unchanged | |
2. | Acetic acid | Unchanged | Unchanged | |
3. | Nitric acid | Unchanged | Dissolve | |
4. | Sulphuric acid | Unchanged | Dissolve | May be cotton |
Confirmation test:
Obs. no. | Chemical | Behavior | Result | |
Cold | Hot | |||
1. | Sulphuric acid | Unchanged | Dissolve | Cotton |
Sample_03
Visual properties:
- Color: White
- Handle: Soft.
Physical test:
Preliminary sorting test by heating:
We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:
Obs. no. | Behavior | Remark |
1. | Shrink from flame or melts with the formation of bead | Thermoplastic |
For thermoplastic fiber:
Bring a small tuft of fibers into a small non-luminous flame –
Obs. no. | Behavior | Odor | Residue | Remark |
1. | Melts then burns (smoky flame) | Aromatic | Glossy brown bead (not crushable) | May be Polyester |
Chemical test:
Obs. no. | Chemical | Behavior | Remark | |
Cold | Hot | |||
1. | Sulphuric acid | Unchange | Unchange | |
2. | Dimethyl formamide | Unchange | Unchange | |
3. | Phenol | Unchange | Dissolve | May be Polyester |
4. | Sodium hydroxide | Unchange | Unchange |
Confirmation test:
Obs. no. | Chemical | Behavior | Result | |
Cold | Hot | |||
1. | Phenol | Unchange | Dissolve | Polyester |
Sample_04
Visual properties:
- Color: Bluish white
- Handle: Soft
Physical test:
Preliminary sorting test by heating:
We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:
Obs. no. | Behavior | Remark |
1 | Shrink from flame or melts with the formation of bead | Thermoplastic |
For non- thermoplastic fiber:
Bring a small tuft of fibers into a small non-luminous flame –
Obs. no. | Behavior | Odor | Residue | Remark |
1 | Fuses then burns (smoky flame) | Sweetish | Dark color Hard bead but brittle | May be Acrylic |
Chemical test:
Obs. no. | Chemical | Behavior | Remark | |
Cold | Hot | |||
1. | Phenol | Unchanged | Color change | |
2. | Dimethyl formamide | Unchanged | Dissolve | May be acrylic |
3. | Nitric acid | Unchanged | Unchanged | |
4. | Sulphuric acid | Unchanged | Dissolve | May be acrylic |
Confirmation test:
Obs. no. | Chemical | Behavior | Result | |
Cold | Hot | |||
1. | Dimethyl formamide | Unchanged | Dissolve | Acrylic |
Conclusion:
I would like to thank our respected teacher for the important instructions. I am also grateful to our lab assistants for their kind help. This experiment helps me to know about the physical and chemical properties of textile fiber that is very important for textile testing. I think this will be very helpful in my future life.
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Founder & Editor of Textile Learner. He is a Textile Consultant, Blogger & Entrepreneur. Mr. Kiron is working as a textile consultant in several local and international companies. He is also a contributor of Wikipedia.