Identification of Textile Fiber | Identification of Thermoplastic Fiber | Fibre Identification

Last Updated on 01/08/2024

Name of the Experiment:
Identification of given textile fiber sample.

Introduction:
The identification of textile fibers is a task frequently performed in a textile lab. The need to identify fibers arises in fibers research as well as during fabric production and processing. The identification of an unknown fiber in a yarn or fabric made up of a mixture of fibers is also often carried out. Identification tests are performed by utilizing tests that take advantage of the different chemical (and to some extent physical) characteristics of textile fibers.

The properties of the yarn and fabric are directly influenced by the properties of fiber from which yarn and fabric are made. There are different methods of fibre identification for characterization of the structural, physical, and chemical properties of fibers. Several methods are used to identify fibers and to differentiate them from one another. The most common methods include microscopic examination, solubility tests, heating and burning characteristics, density or specific gravity, and staining techniques. In this experiment I will discuss identification of thermoplastic and non thermoplastic textile fiber.

Identification of Textile Fiber

Objectives:

  1. To know about the physical properties of textile fiber sample.
  2. To know about the chemical properties of textile fiber sample.
  3. To identify the type of sample fiber.

Sample_01

Visual properties:

  • Color: White
  • Handle: Harsh

Physical test:

Preliminary sorting test by heating:

We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:

Obs. no.BehaviorRemark
1Does not shrink from flame or meltNon-thermoplastic

For non- thermoplastic fiber:
Bring a small tuft of fibers into a small non-luminous flame –

Obs. no.BehaviorRemark
1Burn with irregular spurting flame, leaving a black inflated, easily powdered residue & emits a smell of burnt hair.Protein (Silk & Wool)

Chemical test:

Obs. no.ChemicalBehaviorRemark
ColdHot
1.PhenolUnchangedUnchanged
2.Dimethyl formamideUnchangedUnchanged
3.Sulphuric acidUnchangedDissolveMay be silk
4.Sodium hydroxideUnchangedDissolveMay be wool

Confirmation test:

Obs. no.ChemicalBehaviorResult
ColdHot
1.Sodium hydroxideUnchangedDissolveWool

Sample_02

Visual properties:

  • Color: White
  • Handle: Soft handle

Physical test:

Preliminary sorting test by heating:

We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:

Obs. no.BehaviorRemark
1.Does not shrink from flame or meltNon-thermoplastic

For non- thermoplastic fiber:
Bring a small tuft of fibers into a small non-luminous flame –

Obs. no.BehaviorRemark
1.Burns readily and without melting, emitting a smell of burnt paper & leaving a small amount of ash.Cellulose & Regenerated Cellulose

Chemical test:

Obs. no.ChemicalBehaviorRemark
ColdHot
1.PhenolUnchangedUnchanged
2.Acetic acidUnchangedUnchanged
3.Nitric acidUnchangedDissolve
4.Sulphuric acidUnchangedDissolveMay be cotton

Confirmation test:

Obs. no.ChemicalBehaviorResult
ColdHot
1.Sulphuric acidUnchangedDissolveCotton

Sample_03

Visual properties:

  • Color: White
  • Handle: Soft.

Physical test:

Preliminary sorting test by heating:

We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:

Obs. no.BehaviorRemark
1.Shrink from flame or melts with the formation of beadThermoplastic

For thermoplastic fiber:

Bring a small tuft of fibers into a small non-luminous flame –

Obs. no.BehaviorOdorResidueRemark
1.Melts then burns (smoky flame)AromaticGlossy brown bead (not crushable)May be Polyester

Chemical test:

Obs. no.ChemicalBehaviorRemark
ColdHot
1.Sulphuric acidUnchangeUnchange
2.Dimethyl formamideUnchangeUnchange
3.PhenolUnchangeDissolveMay be Polyester
4.Sodium hydroxideUnchangeUnchange

Confirmation test:

Obs. no.ChemicalBehaviorResult
ColdHot
1.PhenolUnchangeDissolvePolyester

Sample_04

Visual properties:

  • Color: Bluish white
  • Handle: Soft

Physical test:

Preliminary sorting test by heating:

We took small tuft of fibers hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:

Obs. no.BehaviorRemark
1Shrink from flame or melts with the formation of beadThermoplastic

For non- thermoplastic fiber:
Bring a small tuft of fibers into a small non-luminous flame –

Obs. no.BehaviorOdorResidueRemark
1Fuses then burns (smoky flame)SweetishDark color

Hard bead but brittle

May be Acrylic

Chemical test:

Obs. no.ChemicalBehaviorRemark
ColdHot
1.PhenolUnchangedColor change
2.Dimethyl formamideUnchangedDissolveMay be acrylic
3.Nitric acidUnchangedUnchanged
4.Sulphuric acidUnchangedDissolveMay be acrylic

Confirmation test:

Obs. no.ChemicalBehaviorResult
ColdHot
1.Dimethyl formamideUnchangedDissolveAcrylic

Conclusion:
I would like to thank our respected teacher for the important instructions. I am also grateful to our lab assistants for their kind help. This experiment helps me to know about the physical and chemical properties of textile fiber that is very important for textile testing. I think this will be very helpful in my future life.

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